Laboratory Vacuum Freeze Dryer Machine

• Type: Freeze Drying Equipment
• Application: Powder
• Fuel: Gas
• Operating Pressure: Vacuum
• Roller Number: Multi-Drum
• Cloth Membrane Forms: Top Feed
• Model NO.: 12A
• Fluid Bed Drying Equipment Type: Multilayer Fluid Bed
• Vacuum Drying Equipment Type: Continuous Vacuum
• Condition: New
• Customized: Non-Customized
• Structure: Desktop
• Material: Stainless Steel
• Certification: CE, ISO
• Freeze Drying Area: 0.12 Square
• Condenser Capacity: 3-4 L /24h
• Vacuum Degree: < 10 PA
• Dimension: 460*625*(370+430) mm
• Transport Package: Export Standard Packing
• Specification: ce
• Trademark: NANBEI
• Origin: Zhengzhou, Henan, China
• HS Code: 8438600000
• Production Capacity: 10000 Set

Product Description

Vacuum freeze dryer

Product Description

Product features

1. High quality equipment and matching solutions were provided.Different system functions and components configuration can be customized in order to meet different users' needs.
2. The parts were compacted for the modular design, so the equipment was easy to maintain and operate.
3. The interface of the control system was friendly, the operation was convenient and the function was powerful.
4. It was highly close to the principles of production machines.
5. Configuration parts of well-known brands at home and abroad were used.
6. The treatment of parts surface is meeting or exceeding the relevant national or industry regulations.
7. AII interfaces shall be flange mounted.
8. All kinds of sensors were equipped.Timely alarm and active protection will be took when the  function of the equipment were abnormal.
9. In order to easily operate in the clean room, external drying box can be connected for the small experimental freeze -drier.
10. Pilot freeze-drier was designed in accordance with the national pharmaceutical machinery industry standard.
     
    Control system
    The control system was composed of programmable logic controller, man-ma-chine interface device, sensor, terminal relay and digital to analog conversion module. The industrial intelligent  control software was based on professional programmable controller and developed by advanced   configuration configuration software for vacuum freeze-drying equipment.It was that can  display the system status, process flow, alarm point and operation situation of each component,      and can be monitored remotely.

1. It can automatically control the whole freeze-drying process with one key,and also can realize the freeze-drying process manually;
2. The system can show a variety of language interfaces such as Chinese and English    [Russian, India (export optional)]. The system vacuum can be freely converted at mbar, Pa and  Torr. The temperature can be expressed in degrees Celsius and Fahrenheit ;
3. During the operation, the system can automatically monitor and detect and record and store the relevant data. It can also be monitored by remote systems ;
4. From freeze-drying process to defrosting process, all materials can be programmed    automatically and many programs can be stored ;
5. The system was equipped with variety sensors, it can alarm immediately during the  operation of abnormal temperature or pressure, and take active protection to ensure safe and stable operation ;
6. Many data such as real-time-record of vacuum,cold trap temperature, material temperature, shelf temperature, operation error alarm were in this system ;
7. Data was recorded once a minute with freeze-drying curve. The system can record real-time   data continuously and has USB data storage serial port ;
8. The freeze-drying process was recorded, the freeze-drying curve was drawn and the eutectic   point test was achieved ;
9. The man-machine interface equipment of the control system can work stably in the  environment from -20 to 65 degrees Celsius. It conforms to the NEMA (International      Electric Manufacturing Association) protection regulations and the European CE Electrical  Certification standards ;
10. Automatic vacuum regulation was achieved in this system.
     
    Freeze-drying process
    The freeze-drying cycle system consists of intermediate medium, circulating pump, heater,plate heat exchanger, freeze-drying chamber, shelf and pipeline. The freezing and heating of materials   are completed with this system.

1. The freeze-drying process was managed. A number of mature and safe freeze-drying process  were stored in the management system. Users can make up for different products of  freeze-drying process when they adjusted freeze -drying process data;
2. Material can be observed and the freeze-drying parameters can be adjusted at any time in the freeze-drying process;
3. The freeze-drying chamber can effectively pre-freeze the material, and it is suitable for various serum bottles or vials;
4. PID algorithm is used in the automatic control. Materialscan be repeated freeze quickly or slowly;
5. The temperature was even by accurately controlling the medium circulating in the shelf  heating system and the shelf was smooth with the special process. The quality of freeze drying   and the drying efficiency were improved;
6. In order to avoid the contamination of the material after freeze drying, the protection system can be filled with pure nitrogen gas or other protective gas through the system;
7. The gland system can perform manual or automatic accurate and reliable sealing of the material container in the freeze-drying chamber in a vacuum state, the container lid and the container can be reliably sealed;
8. The ice condenser can be defrosted rapidly through the defrost system after freeze-drying  process so as to freeze the material again.
    
   Vacuum system
   The system is composed of vacuum pump or roots pump (optional), freeze- drying box,   vacuum gauge, pipeline and controller. The vacuum pump was equipped with redundancy.

1. The vacuum degree was controlled by PID mode, and the whole automatic control can be realized;
2. Systematically standardized test procedures were took in order to avoid potential vacuum leaks;
3. A device at the suction port of the vacuum pump was provided to prevent the gas flowing back when the equipment was stopped. An oil mist filtering device at the exhaust port is provided to prevent the exhaust gas polluting the surrounding environment;
4. The vacuum can be adjusted automatically or manually. The efficiency of the heat transfer   and freeze drying was increased and the equipment and energy consumption was reduced;
5. The butterfly valve of the pilot freeze-drier between the freeze-drying chamber and the ice condenser should be closed before freeze-drying preparation and the terminative process. So the  material can be handled and pre-frozen in a clean environment.
    
   Refrigeration system
   The utility model was composed of a refrigeration compressor, a condenser and an expander, etc. An imported compressor was adopted in the system. The shelf and the water catcher were  respectively cooled by the slicon oill and the condensing pipe. The system was simple and  reliable. The cold capacity was enough also.The environment-friendly refrigerant was used in  the system. The system can be delay started and automatic controlled.
    
   Selection Guide
   Drying chamber device

1. Standard type: Suitable for bulk (powder, granule, solution) materials before freeze-drying.
2. Gland type: Suitable for freeze-dried materials filled into vials.
3. Multi-manifold type: Suitable for external bottled materials in eggplant-shaped bottles and jars, and freeze-drying multiple varieties at the same time.
4. Type T: Suitable for freeze-dried materials in ampoule tubes.
   Optional accessories

1. Multi-manifold bottle hanging device, lyophilized bottle (eggplant-shaped bottle and jar), ampule tube lyophilized rack
2. Imported vacuum pump, high-speed vacuum pump oil, vacuum pump exhaust port oil mist filter, vacuum pump intake port dust filter
3. Ampoule tube sealer, Vial capping machine
4. Eutectic point tester, inert gas filling port
5. Stainless steel two-story experimental trolley

Detailed Photos

Product Parameters

Experimental type  Pilot type																	Production type
Model	Unit	12A	10C	10E	25C	25E	15E	22E	30E	20G	30G	40G	50E	80E	100E	120E	200	300	500
Effective partition area	m^2	0.12	0.1		0.25		0.15	0.22	0.3	0.2	3	0.4	0.5	0.8	0.98	1.22	2.16	3.24	5.67
Water catching capacity	Kg	2	3		6		7			8			15		20		50	60	5.67
22 mm vial	bottle	110	110		390		336	504	672	448	672	870	980	1450	2160	2700	4800	7500	13300
16 mm vial	bottle	200	200		759		638	927	1276	851	1240	1650	1870	2800			9200	14000	25200
Partition size	mm	Φ180					312x 242			335 x 300			300x 420	320x500	405x 605		600x 600	600x 900	900 x 900
(Length x width)		Φ170	®180		Φ277
Available partitions	pcs	5	4				2	3	4	2	3	4	4	5	4	5	6+1		7+1
Interlayer spacing	mm	70	50	45	76	70	143	90	65	143	90	65	68	90	100	76	100
Standard cold trap temperature	ºC		-60 Ambient temperature≤30)		-62 (Ambient temperature≤30)		-80(Ambient temperature≤30)
Ultimate  cold trap temperature	ºC	≤-47	-65(Ambient temperature≤25)		-65(Ambient temperature≤25)		-83 (Ambient temperature≤25)										≤-70 (Ambient temperature≤30)
Standard vacuum	Pa	5(no- load)	5(no- load)		5(no- load)		10(no- load)										10(no- load)
Ultimate vacuum	Pa	1(no- load)	1(no- load)		1(no- load)		1(no- load)										≤10(no- load)
Shelf temperature range	ºC			Electric heating(50)		Electric heating(50)	-50-+70										-50-+70
Dimensions	mm	540 x 540 x 370	610x 610 x460		640x540x845		650x700x1288				700x800x 1550		1520x730x1400	1490x 780x 1710	2000 x 950x 1700
Length X Width X Height
Applicable power supply		AC220V 50HZ					AC380V 50HZ Three-phase five-wire system(OptionalAC220V 50HZ)						AC380V 50HZ  Three-phase five-wire system
Total power	W	1000	1250	1400	1900	2150	3300						4200		8600		18000	21000	25000
Weight	Kg	55	85		120		250	255	260	290	295	300	650	750	1300
Applicable environment	ºC	Ambient temperature≤30

 

Experimental type  Pilot type

Production type

Model

12A

10C

10E

25C

25E

15E

22E

30E

20G

30G

40G

50E

80E

100E

120E

200

300

500

Pre-freezing function

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Partition silicone oil cooling and heating

N

Y

Y

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Accurate temperature control of the partition

N

N

N

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Controllable heating rate

N

N

N

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Upgradable PLC control system

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Color touch screen

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Automatic control

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Partition electric heating

N

A

Y

N

Y

A

A

A

N

N

N

A

A

N

N

A

A

A

Display freeze-drying curve and data

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

The upper computer monitors the lower computer

N

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Wireless connection remote control

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Large-capacity data storage

N

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Cold trap automatic defrosting

N

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Controllable vacuum

N

N

N

N

N

A

A

A

A

A

A

A

A

A

A

A

A

A

Capping system

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Eutectic point test

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

CMP clean room installation

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Air cooling

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

N

N

N

Multi-manifold device

A

A

A

A

A

A

A

A

A

A

A

N

N

N

N

N

N

N

T-frame for ampoules

A

A

A

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Freeze-drying endpoint test

N

N

N

N

N

N

N

N

A

A

A

A

A

A

A

A

A

A

Circulating water cooling

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Y

Y

Y

Online disinfection

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

A

A

A

Online cleaning

N

N

N

N

N

N

N

N

N

N

N

N

N

A

A

A

A

A

Technical features listYIndicates that it has the function  AIndicates optional  ○Indicates that the function is not applicable
Remark: This product is for civilian use only

Certifications

Packaging & Shipping

Company Profile

FAQ

FAQ     

1. How can I choose the suitable one?
Dear customer, please tell us your detailed requirements by mail or online, we will recommend the suitable one as your request.
2. Does your price is competitive?
Dear customer, we make sure to offer you the best quality with competitive price.
3. How can I pay?
Dear customer, we accept many payment term, such as T/T, Western Union…
4. When I receive it after pay?
Dear customer, normal models can be delivered with 5-7days, please contact us to check transport time to your address.
5. How to deliver?
Dear customer, we can send by Express, by Sea and by Air.
6. Is will be broken during transport?
Dear customer, please do not worry, we do standard export package.
7. What should I do if I do not know how to use?
Dear customer, please do not worry, manual user will be sent together, you can also contact us with more technological support.
8. What should I do if some parts broken?
Dear customer, please do not worry, we have 12months warranty except  wear parts. You can also buy parts from us after 12months.

Pre-sale service
· 24hours online to ensure quick response to customers' inquiry or online message;
· Guide customers to choose the best suitable machine model;
· Offer detailed specification and competitive prices;
Contract execution
· Machine production will be arranged strictly according to the contract;
· Machine photos will be sent to you for inspection during production;
· Send customs clearance documents by DHL;
· Update latest news after delivery and prepare customs clearance;
After-sale service
· 12 months warranty except for wear parts;
· Broken spare parts (except for wear parts) will be sent for free due to quality problems;
· In time response to customers technical problems;
· New products update for customers' reference

Our Company:
Since 2008, We have become a professional laboratory instrument manufacturer.
Since the establishment of the International Department in 2010, the products are exported to Europe, America and Asia and Africa!
Whether it is technology, factory area, multi-language sales. We are all professional!